Synthesis and Characterization of Amphiphilic Iron-Sulfur Core Dendrimers

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dc.contributor.advisorDaniel L. Feldheim, Committee Memberen_US
dc.contributor.advisorEdmond F. Bowden, Committee Memberen_US
dc.contributor.advisorChristopher B. Gorman, Committee Chairen_US
dc.contributor.authorDembowa, Anetaen_US
dc.date.accessioned2010-04-02T18:11:41Z
dc.date.available2010-04-02T18:11:41Z
dc.date.issued2005-07-31en_US
dc.degree.disciplineChemistryen_US
dc.degree.levelthesisen_US
dc.degree.nameMSen_US
dc.descriptionNorth Carolina State University Theses Chemistry.
dc.description.abstractSynthesis of water soluble carboxylate-terminated Fe4S4-core was carried out. Convergent method was chosen to build three generations of dendrons. Several synthetic schemes were explored. The syntheses were conducted with 4,4-bis(hydroxyphenyl)penthanol as a repeat unit and N,N-dimethyl thiocarbamate and methyl ester or methoxy-methyl as protecting groups. The conditions for deprotection and ligand exchange have been proposed. 1H, 13C and MALDI-MS were used to characterize synthesized molecules.en_US
dc.formatThesis (M.S.)--North Carolina State University.
dc.identifier.otheretd-01022005-192535en_US
dc.identifier.urihttp://www.lib.ncsu.edu/resolver/1840.16/2249
dc.rightsI hereby certify that, if appropriate, I have obtained and attached hereto a written permission statement from the owner(s) of each third party copyrighted matter to be included in my thesis, dissertation, or project report, allowing distribution as specified below. I certify that the version I submitted is the same as that approved by my advisory committee. I hereby grant to NC State University or its agents the non-exclusive license to archive and make accessible, under the conditions specified below, my thesis, dissertation, or project report in whole or in part in all forms of media, now or hereafter known. I retain all other ownership rights to the copyright of the thesis, dissertation or project report. I also retain the right to use in future works (such as articles or books) all or part of this thesis, dissertation, or project report.en_US
dc.subjectDendrimeren_US
dc.subjectEncapsulationen_US
dc.subjectStructure-Property Relationshipsen_US
dc.subjectIron-Sulfur Clusteren_US
dc.titleSynthesis and Characterization of Amphiphilic Iron-Sulfur Core Dendrimersen_US
dcterms.abstractKeywords: Dendrimer, Encapsulation, Structure-Property Relationships, Iron-Sulfur Cluster.
dcterms.extentxii, 156 pages : illustrations (some color)

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