A Dynamically Polarized Deuteron Target

dc.contributor.advisorAlbert R. Young, Committee Memberen_US
dc.contributor.advisorPaul R. Huffman, Committee Memberen_US
dc.contributor.advisorChristopher R. Gould, Committee Chairen_US
dc.contributor.advisorMohamed A. Bourham, Committee Memberen_US
dc.contributor.authorPoole, John Owenen_US
dc.date.accessioned2010-04-02T19:05:19Z
dc.date.available2010-04-02T19:05:19Z
dc.date.issued2007-12-07en_US
dc.degree.disciplinePhysicsen_US
dc.degree.leveldissertationen_US
dc.degree.namePhDen_US
dc.description.abstractA dynamically polarized deuteron target was constructed at the Triangle Universities Nuclear Laboratory for low energy polarized neutron transmission experiments. Theoretical calculations suggested a measurement of the longitudinal spin-dependent total $vec[n]-vec[d]$ cross section difference, $Deltasigma_L$, would provide evidence of three nucleon force effects. The target was operated at a temperature of 0.5K with a recirculating $ˆ3$He evaporation refrigerator and a 2.5T split-pole superconducting magnet which can be mechanically mounted to produce either a longitudinally or tangentially polarized target relative to the beam momentum. The target material consisted of a cube of volume 2.7 ml of either partially (D6) or fully (D8) deuterated 1,2-propanediol chemically doped with EHBA-Cr$ˆV$ to provide the paramagnetic centers for dynamic nuclear polarization with microwaves in the region 69GHz. Polarization was monitored during the experiment using a continuous wave NMR Q-meter capable of both phase sensitive and magnitude detection. A PC running LabVIEW controlled data acquisition, frequency sweep of the digital frequency synthesizer and a novel background cancellation technique. A pre-recorded background signal was subtracted on a channel by channel basis before the NMR spectrum was sampled. Polarization was extracted from the NMR spectra by a fit to a theoretical lineshape. Effects including dispersion were considered. The equal spin temperature (EST) hypothesis was used to determine deuteron polarization indirectly though the measurement of polarization of the residual protons in the partially deuterated sample. Efforts to improve the system stability and signal-to-noise are discussed along with numerical methods, fitting strategy and evaluation of uncertainties.en_US
dc.identifier.otheretd-11092007-143105en_US
dc.identifier.urihttp://www.lib.ncsu.edu/resolver/1840.16/4970
dc.rightsI hereby certify that, if appropriate, I have obtained and attached hereto a written permission statement from the owner(s) of each third party copyrighted matter to be included in my thesis, dis sertation, or project report, allowing distribution as specified below. I certify that the version I submitted is the same as that approved by my advisory committee. I hereby grant to NC State University or its agents the non-exclusive license to archive and make accessible, under the conditions specified below, my thesis, dissertation, or project report in whole or in part in all forms of media, now or hereafter known. I retain all other ownership rights to the copyright of the thesis, dissertation or project report. I also retain the right to use in future works (such as articles or books) all or part of this thesis, dissertation, or project report.en_US
dc.subjectNMR polarimetryen_US
dc.subjectdynamic nuclear polarizationen_US
dc.subjectfit to NMR spectraen_US
dc.subjectdynamically polarized deuteron targeten_US
dc.titleA Dynamically Polarized Deuteron Targeten_US

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